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Beilstein J. Org. Chem. 2016, 12, 1111–1121, doi:10.3762/bjoc.12.107
Graphical Abstract
Figure 1: Modular concept for manzacidin synthesis based on a Tsuji–Trost coupling of joint intermediate 5.
Scheme 1: General concept for heterocycles synthesis based on a nucleophilic addition and Tsuji–Trost couplin...
Scheme 2: Synthesis of homoallylic alcohol 12 by multi-component reactions.
Scheme 3: Preparation of urea-type cyclization precursor 19.
Scheme 4: Stereodivergent synthesis of 1,3-syn- and anti-tetrahydropyrimidinones [31].
Scheme 5: Stereoselective synthesis of all possible stereoisomers of the manzacidin core amine by asymmetric ...
Scheme 6: Synthesis of the authentic cyclization precursor 5.
Figure 2: X-ray structure of 39.
Scheme 7: Divergent Tsuji–Trost coupling and completion of the synthesis of authentic pyrimidinones 3 and 4.